Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A

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For example, many low-carbon and stabilized stainless steels e. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance.

A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results. Share on Tumblr Print. Please specify the maximum practtice corrosion rate and any available data on the sensitizing heat treatment performed.

At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type.

ASTM A Testing: An Overview of Intergranular Corrosion | Element

The level of corrosion is determined by mass loss. This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility.

In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. Discover perspectives, resources, and advice from our world-leading Engaged Experts. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.


Intergranular Corrosion Testing: An Overview of ASTM A262

The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated. The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.

Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

This method is a hour boiling test for “as received” specimens of stainless steel. This method is preferable for chromium depletions and corrosion in intermetallic phases. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. What is your typical turnaround time?

The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. See Appendix X1 for information regarding test selection.

Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: Like what you saw? By using our website you consent to all cookies in accordance with our Cookie Policy.

ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. To understand intergranular corrosion testing or wstm attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.


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Because it can be run quickly for screening, we often run this test first. Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges.

The etch structure types used to classify the pracrice are: Practice A, the oxalic acid etch test is used as a rapid technique to screen samples practics certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.

This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. The Oxalic Acid test is only used to ensure that no corrosion practuce samples are labeled either “Acceptable” or “Suspect”. Methods for preparing the test adtm, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.

Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels.